Caricature Studio 3.6 Crack Serial 13 [TOP]
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Caricature Studio 3.6 Crack Serial 13
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A rapid, simple and sensitive high-performance liquid chromatography-tandem mass spectrometry method was developed and validated for the simultaneous determination of levosulpiride and metoclopramide in human plasma using rosuvastatin (internal standard, IS) for the first time. Liquid-liquid extraction was applied to plasma samples using methyl tert-butyl ether. Chromatographic separation was performed on a Phenomenex Synergi Fusion-RP 80 Å (150 x 3 mm, 4 microm) column using 5 min run time. The mobile phase consisted of methanol-0.1% formic acid (70:30, v/v), and was pumped at a flow rate of 0.5 ml/min. The analytes were ionized in the positive mode via an electrospray ionization source. Multiple reaction monitoring, using the transitions m/z 270.3–>162.1 for metoclopramide and m/z 321.2–>200.1 for levosulpiride, was used for the quantification. The linear range for levosulpiride and metoclopramide in human plasma was 0.10-10.0 and 0.25-10.0 ng/ml, respectively (r > 0.9900). The intra- and inter-day accuracies were within +/-10%, and the corresponding precisions were Q:
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